1st Edition

Materials Characterization Techniques

By Sam Zhang, Lin Li, Ashok Kumar Copyright 2008
342 Pages 208 B/W Illustrations
by CRC Press

344 Pages
by CRC Press

Experts must be able to analyze and distinguish all materials, or combinations of materials, in use today—whether they be metals, ceramics, polymers, semiconductors, or composites. To understand a material’s structure, how that structure determines its properties, and how that material will subsequently work in technological applications, researchers apply basic principles of chemistry, physics,... Read more

Preface

Introduction

Contact Angle in Surface Analysis

Measuring Contact Angle

Determining Surface Energy of a Homogeneous Solid Surface

Work Examples

X-ray Photoelectron Spectroscopy and Auger Electron Spectroscopy

Atomic Model and Electron Configuration

Principles of XPS and AES

Instrumentation

Routine Limits of XPS

XPS Applications and Case Studies

AES Applications

Scanning Tunneling Microscopy and Atomic Force Microscopy

Working Principle

Instrumentation

Modes of Operation

Differences between STM and AFM

Applications

X-ray Diffraction

X-ray Characteristics and Generation

Lattice Planes and Bragg’s Law

Powder Diffraction

Thin Film Diffraction

Texture Measurement

Grazing Angle X-ray Diffraction

Transmission Electron Microscopy

Basics of Transmission Electron Microscopes

Reciprocal Lattice

Specimen Preparation

Bright-Field and Dark-Field Images

Electron Energy Loss Spectroscopy

Scanning Electron Microscopy

Introduction to Scanning Electron Microscopes

Electron Beam–Specimen Interaction

SEM Operating Parameters

Applications

Chromatographic Methods

General Principles of Chromatography

Ion Exchange Chromatography

Gel Permeation Chromatography

Gel Electrophoresis Chromatography

High-Performance Liquid Chromatography

Gas Chromatography

Quantitative Analysis Methods

Infrared Spectroscopy and UV/Vis Spectroscopy

Infrared Radiation Spectroscopy

Ultraviolet/Visible Spectroscopy

Macro and Micro Thermal Analyses

Macro and Micro Differential Scanning Calorimetry

Isothermal Titration Calorimetry

Thermogravimetric Analysis

Laser Confocal Fluorescence Microscopy

Fluorescence and Fluorescent Dyes

Fluorescence Microscopy

Laser Confocal Fluorescence Microscopy

Applications of LCFM

Index

Biography

Sam Zhang, Lin Li, Ashok Kumar