This textbook is a comprehensive guide to analysis of carbohy-drates by gas-liquid chromatography and mass spectrometry. In addition to explaining the facets of carbohydrate analysis and their relation to each other, the text also contains in-depth reference in-formation useful to practitioners in the field. Improvements in car-bohydrate analyses methodology during the past six years are also highlighted. This extensively illustrated text provides excellent data for those in carbohydrate, agriculture, and food chemistry.
Table of Contents
1. Introduction to Analysis of Carbohydrates by Gas-Liquid Chromatography (GLC) 2. High-Performance Liquid Chromatography (HPLC) of Carbohydrates 3. Hydrolysis and Other Cleavage of Glycosidic Linkages 4. Silyl Ethers of Carbohydrates 5. Preparation of Alditol Acetates and Their Analysis by Gas Chromatography (GC) and Mass Spectrometry (MS) 6. Analysis of Monosaccharides as Per-O-Acetylated Aldononitrile (PAAN) Derivatives by Gas-Liquid Chromatography (GLC) 7. Carbohydrate Trifluoroacetates 8. Analysis of Carbohydrates as O-Alkyloxime Derivatives by Gas-Liquid Chromatography (GLC) 9. Linkage Structure of Carbohydrates by Gas Chromatography-Mass Spectrometry (GCMS) of Partially Methylated Alditol Acetates 10. Fast Atom Bombardment-Mass Spectrometry (FAB-MS): Sample Preparation and Analytical Strategies 11. Location of Cellulose Substituents 12. Miscellaneous Gas Chromatographic (GC) Analyses of Carbohydrates
Biermann, Christopher J.; McGinnis, Gary D.